Image of PENGARUH TEMPERATUR KALSINASI TERHADAP KARAKTER SILIKA ZIRCONIUM TERSULFATASI DENGAN TEMPLATE EDTA DAN APLIKASINYA UNTUK DEHIDRASI ISOPROPIL ALKOHOL

Skripsi

PENGARUH TEMPERATUR KALSINASI TERHADAP KARAKTER SILIKA ZIRCONIUM TERSULFATASI DENGAN TEMPLATE EDTA DAN APLIKASINYA UNTUK DEHIDRASI ISOPROPIL ALKOHOL

Penilaian

0,0

dari 5
Penilaian anda saat ini :  

In this study ZrSO4-SiO2 catalyst with EDTA template was used as a catalyst which was synthesized by calcination method. The preparation of sulphated zirconium impregnated silica catalyst was carried out at various temperatures, such as 400°, 500°, 600°, 700° and 800°C. This study aims to determine how the temperature of the catalyst ZrSO4-SiO2 EDTA template influences. The XRD results on the ZrSO4-SiO2 catalyst variation 3 600°C, at an angle of 22.46° have an amorphous shape characterized by a widened peak. While at 400° and 800°C, several peaks appeared at an angle of 2θ, namely 22.30°, with a sharp peak with high intensity at an angle of 21.989°C indicating that there is a cristobalite structure. The results of the characterization of the catalyst using FT-IR at wave numbers 3443.25 cm-1, 3425.06 cm-1 and 3411.27 cm-1 showed the stretching vibration of –OH groups from Si-OH. The results of the GC-MS analysis showed that the selectivity of the ZrSO4-SiO2 catalyst was highest at 800°C with a value of 77.7%. Meanwhile, the highest conversion value was found at 400°C with a value of 44.45% and the ZrSO4-SiO2 catalyst at 800°C gave the highest yield value of 34.7%.

Availability
Inventory Code Barcode Call Number Location Status
2407001384T140147T1401472024Central Library (References)Available but not for loan - Not for Loan
Detail Information
Series Title
-
Call Number
T1401472024
Publisher
Inderalaya : Prodi Ilmu Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam.,
Collation
ix, 30 hlm.; ilus.; tab.; 21 cm.
Language
Indonesia
ISBN/ISSN
-
Classification
540.07
Content Type
Text
Media Type
-
Carrier Type
-
Edition
-
Subject(s)
Prodi Ilmu Kimia
Dehidrasi Alkohol
Specific Detail Info
-
Statement of Responsibility
Other version/related

No other version available

File Attachment
Comments
You must be logged in to post a comment