Skripsi

PENGARUH KOMPOSISI GLUKOSA DAN ZEOLIT TERHADAP SIFAT KATALIS KOMPOSIT ZEOLIT-KARBON SULFONAT

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Penilaian

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The research of influence of glucose and zeolite to charasteristic of catalytic composite of zeolite-carbon sulfonic was done. Heterogeneous catalysts based on sulfonate carbon was made by mixing glucose and zeolit with ratio composition 1:3, 1:2, 1: 1,2: 1 and 3: 1. Carbonisation procces was done at 400°C during 15 hours and followed sulfonated by using sulfuric acid during 4 hours at 175°C. The result of catalytic on esterification reaction glacial asetat acid and ethanol showed that composition 1:3 has highest yield ettyl acetat of 91.294%. Analysis data GCMS showed the mayor product of esterification reaction was a ethyl asetat (C4II8O2) vvilth molccular at m/z 88 . The highest sum acidity value us mucli as 9.4 mmol/g strenghted that 1:3 composition was the best composition. Characteritation of catalyst by using SEM-EDX and FT-IR spectrofotometer. SEM-EDK analyst showed solface topology of zeolit was conted by sulfonatecarbon wich showed with vibaration of sulfur at 2.307 keV. FT-IR spetra showed a vibration of sulfonate group (-SO3H) at wave number 1080 cm was active side catalyst. Based on the research it can be concluded that the catalytic composite of zeolite-carbon sulfonic can be used in the esterification reaction and showed the optimal catalytic activity. The more glucose as carbon source. the catalvtic activitv will increase.

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Availability

Inventory Code	Barcode	Call Number	Location	Status
1407004150	T71091	T710912014	Central Library (Referens)	Available but not for loan - Not for Loan

Detail Information

Series Title

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Call Number

T710912014

Publisher

Inderalaya : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Sriwijaya., 2014

Collation

xv, 51 hlm.; ill.; tab.; 28 cm.

Language

Indonesia

ISBN/ISSN

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Classification

541.307

Content Type

Text

Media Type

unmediated

Carrier Type

unspecified

Edition

-

Subject(s)

Kimia
Ziolit--Karbon Sulfonat

Specific Detail Info

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Statement of Responsibility

HALIM

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