Skripsi

ISOLASI DAN IDENTIFIKASI SENYAWA METABOLIT SEKUNDER EKSTRAK ETIL ASETAT BATANG TUMBUHAN BROTOWALI (Tinospora crispa L)

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Penilaian

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Secondary metabolite from ethyl acetate extract of Tinospora crispa stems has been isolated. The extraction was done by maceration, while the separation and purification of isolated compound was done by chromatographic technique. Structural determination of isolated compound was based on the analysis of spectroscopic data of ‘H NMR, l3C NMR, DEPT and compared to literature data. The isolated compound was in the form of white crystals with melting point of 126°C -128 °C. 'H-NMR spectrum showed signals for vinylic and aliphatic specific for steroids compound. 13C-NMR spectrum showed 29 carbon atom signals which were the signal of 2 methilene (CH2) and 27 signals of methyl groups (CH3). According to DEPT spectrum the 29 signals of carbon atom consisted of 3 quatemary carbon signals, 11 tertiary carbon signals (CH), 9 secondary carbon signals (CH2), and 6 primary carbon signal (CH3). Based on the analysis of spectroscopic data and on comparing data to literature, it was concluded that the isolated compound was steroids namely (3-sitosterol with molecular formula C29H50O BM 414 g/ mol.

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Availability

Inventory Code	Barcode	Call Number	Location	Status
1407002367	T71277	T712772014	Central Library (Referens)	Available but not for loan - Not for Loan

Detail Information

Series Title

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Call Number

T712772014

Publisher

Inderalaya : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Sriwijaya., 2014

Collation

xvi, 46 hlm.: Ilus., tab.; 28 cm

Language

Indonesia

ISBN/ISSN

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Classification

541.307

Content Type

Text

Media Type

unmediated

Carrier Type

unspecified

Edition

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Subject(s)

Kimia
Batang Brotowali

Specific Detail Info

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Statement of Responsibility

HALIM

Other version/related

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