Skripsi
PREPARASI DAN KARAKTERISASI NANOMATERIAL BERBASIS POLIOKSOMETALAT TIPE KEGGIN H4[a-SiW12O40].nH2O DENGAN PENGEMBAN Si02, Ti02, ZrOCl2 dan TaCl.
Preparation of nanomaterial based on polyoxometalate with Si02, Ti02, ZrOCl2 and TaCI to form nanomaterial H4[a-SiWi204o]-nH20-Si02, H4[a-SiWi2O40].nH2O-TiO2, H4[a-SiW,2O40].nH2O-ZrOCl2 and H4[a-SiWi2O40].nH2Ota has been carried out. Nanomaterials were characterized using FT-IR, XRD and SEM. The results of characterization show that nanomaterials ELt[a-SiWi204o].nH20-Si02 and nanomaterial from preparation. The main vibration FT-IR characterization of fiinctional group from H4[a-SiWi204o].nH20-Si02 appared at wevenumbers 462 cm'1, 694 cm'1, dan 1087 cm’1. Nanomaterial H4[a-SiWi204o].nH20-TaCl has vibration at wevenumbers 601 cm’1 and 786cm’1. XRD diffraction pattem for nanomaterials H4[a-SiWi204o].nH20-Si02 and H4[a-SiWi2O40].nH2O-TaCl show both nanomaterials were succesfully supported by metal oxides. The SEM photo analysis of H4[a-SiWi204o].nH20-Si02 and H4[a-SiWi204o].nH20-TaCl show material with nano size. FT-IR spectrum and XRD pattem of EUfa-SiWi204o].nH20 -Ti02 and H4[a-SiWi204o].nH20-ZrOCl2 show supporting of metal oxides Ti02 and ZrOCl2 did not procceded. Nevertheless, SEM photo show H4[a-SiWi204o].nH20-Ti02 and H4[a-SiWi204o].nH20-ZrOCl2 form material with nano size and has homogeneous distribution.
Inventory Code | Barcode | Call Number | Location | Status |
---|---|---|---|---|
1407002361 | T65534 | T655342014 | Central Library (REFERENCES) | Available but not for loan - Not for Loan |
No other version available