Skripsi

APLIKASI KATALIS KOMPOSIT MONTMORILONIT KARBON SULFONAT PADA REAKSI ESTERIFIKASI ASAM ASETAT - ETANOL

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Penilaian

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Research on a heterogeneous catalyst in the form of montmorillonite sulfonated carbon composite has been done. Montmorillonite sulfonated carbon composite was prepared by mixing molasses with montmorillonite and was stirred for 1 hour. Mixture was heated at temperature 120°C for 6 hour to reduce the water content. Mixture was carbonized at temperature of 400°C for 15 hours. The results of carbonization performed sulfonation process at temperature of 175°C for 15 hours. The product of sulfonation was washed with demin water repeatedly until pH neutral. The product was cailed montmorillonite sulfonated carbon composite. Catalyst montmorillonite sulfonated carbon composite performance was tested using acid-base titration method. Montmorillonite sulfonated carbon composite was characterized using FT-IR to study the structure and SEM to study surface topology. Montmorillonite sulfonated carbon composite was applied to the esterification reaction of acetic acid-ethanol and products were identified using GC-MS. Acidity test indicated that the acid number reaches 9.79 mmol g-1. FT-IR showed the presence of sulfonated groups on the 1750 cm'1 and 1087.85 cm'1. SEM EDX was showed that indicate a sulfur atom sulfonate group attached to the composite. The esterification test reached 72.674% of yield.

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Availability

Inventory Code	Barcode	Call Number	Location	Status
1407004151	T65910	T659102014	Central Library (REFERENCES)	Available but not for loan - Not for Loan

Detail Information

Series Title

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Call Number

T659102014

Publisher

Inderalaya : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Sriwijaya., 2014

Collation

xv, 34 hlm.; ill.; tab.; 28 cm.

Language

Indonesia

ISBN/ISSN

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Classification

541.307

Content Type

Text

Media Type

unmediated

Carrier Type

unspecified

Edition

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Subject(s)

Jurusan Kimia
Kimia Fisik

Specific Detail Info

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Statement of Responsibility

Furika

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