Skripsi

TRITERPENOID JENIS LUPANA DARI FRAKSI ETIL ASETAT KULIT BATANG Calophyllum pulcherrimum WALL

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Penilaian

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The triterpenoid compound had been isolated from ethyl acetate fraction from bark of Calophyllum pulcherrimum Wall. Extraction was done with partition method using ethyl acetate and resulted compound was separated using chromatography technique. Compound isolation resulted 0.06 g white crystal, with melting point 213-215 °C. UV spectrum showed maximum absorption at X,max 290 nm (7t->n* trantition) from (-C=C-) and Xmax 342 nm (n—m*) from (-C=0). IR spectrum showed characteristic absorption at wave number omax (cm'1) at 3328.9 cm'1 (OH functional group), 2945.1-2856.4 cm'1 (aliphatic C-H) 1737.7 cm-1 (C=0 functional group), 1637.5 cm'1 (carboxy!ate C-O), 1379.0 cm'1 (gem dimetil), 1041.5 cm'1 (alcohol -C-O). LCMS showed one signal at retention time (T = 3.9 minutes). 'H-NMR spectrum seen existence six signal with 3H integration at 8h 0.75; 0.82; 0.94; 0.96;1.02; and 1.67 ppm and metilen proton (vinilik) at 8h 4.68 ppm (IH, d) and 4.56 ppm (IH, d), furthermore proton signal at 8h 3.18 ppm (IH, t) be individuality from sketch base triterpen cluster that OH. 13C-NMR found three signal 8c 173.7 ppm carbonil signal (-C=0), 151.2 and 109.5 ppm signal (-C=C-), at 8c 79.2 ppm cluster that (-CH-OH), compotmd isolation result be triterpenoid compound kind lupana with molecule formula C3oH4g03.

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Availability

Inventory Code	Barcode	Call Number	Location	Status
1007001088	T65306	T653062010	Central Library (Referens)	Available but not for loan - Not for Loan

Detail Information

Series Title

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Call Number

T653062010

Publisher

Inderalaya : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahan Alam Universitas Sriwijaya., 2010

Collation

xii, 39 hlm.: Ilus., tab.; 28 cm

Language

Indonesia

ISBN/ISSN

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Classification

547.710 7

Content Type

Text

Media Type

unmediated

Carrier Type

unspecified

Edition

-

Subject(s)

Kimia
Kulit Batang Wall

Specific Detail Info

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Statement of Responsibility

HALIM

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